Smartchemsynth Multipurpose High Temperature and High Pressure (SCS-M) Solid-Liquid Reactor

Liquid-Liquid Separator (SCS-LL)

Either working in batch or flow, extractions dealing with liquid-liquid are hectic. This product module in the flow chemistry is equivalent of a separatory funnel. Continuous Liquid-Liquid separation works on the principle of polarity difference. By using advanced membrane technology rather than gravity, this liquid-liquid flow separator can separate two-phase mixtures i.e. into the aqueous layer and organic layer. This system/device can separate liquids with the same density and emulsions with continuous operation. The separator has excellent performance when operated with two liquids with very low interfacial tension.

Our liquid-liquid flow separator delivers:

  • reduced emulsions compared to batch separation funnels,
  • fast partitioning, phase separation and
  • is easy to use.

Internal Layers of Liquid-Liquid Separator

 

Liquid-Liquid Learning Separator 30ml (SCS-LLL-30)

SmartChemSynths Liquid- Liquid Learning Separator Nylon 30ml (SCS-LLL-30N)

SmartChemSynths Liquid-Liquid Learning Separator SS-316 30ml (SCS-LLL-30SS)

 

Liquid-Liquid learning Separator (SCS-LLL-30) Specifications:

  • Pressure: Upto 2 bar
  • Flow rate: up to 30 ml/min
  • Wetted parts: PTFE
  • Dead volume: 700 µL
  • Maximum operating pressure: 1 bar
  • Temperature Range: 25 to 120 oC
  • Membrane: 0.25-0.45-micron PTFE
  • Inlet/Outlet ports: 1/16, 1/8, 1/4ʺ-28 UNF

 

Liquid-Liquid Pilot Separator 200ml (SCS-LLP-200)

SmartChemSynths Liquid- Liquid Pilot Separator SS-316 200ml (SCS-LLP-200SS)

SmartChemSynths Liquid- Liquid Pilot Separator Nylon 200ml (SCS-LLP-200N)

SCS Liquid-Liquid Pilot Separator (SCS-LLP-30) Specifications:

  • Pressure: Upto 2 bar
  • Flow rate: up to 200 ml/min
  • Wetted parts: PTFE
  • Dead volume: 20 mL
  • Maximum operating pressure: 1 bar
  • Temperature Range: 25 to 120 oC
  • Membrane: 0.25-0.45-micron PTFE
  • Inlet/Outlet ports: 1/8, 1/4ʺ-28 UNF


FUNCTION OF LIQUID-LIQUID SEPARATOR:

When a mixture of two liquids enters the separator composed of aqueous liquid and organic liquid, one phase will have an affinity for the membrane and fill the pores this is referred to as the “wetting” phase), and the other phase will be repelled and will not fill the pores this is referred to as the “non-wetting” phase. Once the membrane pores are filled with the wetting phase, a pressure differential is applied between the two sides of the membrane. The separator is designed to maintain a constant pressure differential across the designated flow rates even when conditions are fluctuating. When a hydrophobic membrane is in place, the organic phase passes through the membrane while the aqueous, which is the non-wetting phase, is retained.

Concept:

The concept of liquid-liquid separator is that it exploits differences in wettability and surface forces to accomplish the separation as a result, the device can separate liquids with the same density and emulsions with continuous operation.

ADVANTAGES

  • The separation can be done faster with this liquid separator compared to batch process, and, thus this increases output of product.
  • Continuous separation can be achieved which speeds up the overall separation.
  • Emulsions and rag layers normally take long periods of time to separate leading to inefficiencies.
  • Liquid-liquid separator allows for easy separation of emulsions by removing the matrix fluid and forcing the emulsion to coalesce.
  • Since separation is density independent, even the most challenging emulsions can be separated with ease.

Sunflower Equivalent Solar Panel Micro-Flow Reactor

Sunflower Equivalent Solar Panel Micro-Flow Reactor

The breakthrough Sun-flower equivalent solar panel micro-flow reactor by Smartchemsynths Machine (OPC) Pvt. Ltd. has wrapped up together the advantages of continuous flow processing with the added benefits of ultraviolet light to enable photochemical reactions.

By eliminating the problems encountered in traditional batch photochemistry, this reactor allows the full potential of photochemistry to be exploited. It offers safe, efficient, and scalable photochemistry under continuous flow operation.

The ultimate light source has been used which is the Sun. The lights fall on the solar panel which placed at a fixed angle to absorb maximum intensity of light. The solar reactor panel is placed in an acrylic box. This solar reactor panel is in series with pump control panel.

Features:

  • Chemically inert tube
  • Easy scale-up
  • Efficient, uniform irradiation
  • Safer in operation

Specifications:

M.O.C

Solar reactor: PFA

Setup box: Acrylic

Pumps: Nylon (Customizable)

Reactor vol.

10ml/min – 1l/min, (customization available as per client requirement)

Flow rate

1µl/min – 20µl/min, (customization available as per client requirement)

Temperature

at RT

Pressure

upto 10bar

Solar panel Stand

Each hole at a displacement angle of 100

Recommended Android App. For measuring light intensity

LUX Light Meter.

Multipurpose-High-Temperature-and-High-pressure-sloid---Liquid-Reactor

Smartchemsynth Multipurpose High Temperature and High Pressure (SCS-M) Solid-Liquid Reactor

Specifications of Multipurpose High Temperature and High Pressure (SCS-M) Solid-Liquid Reactor:

    • Smart flow reactor

Multi-purpose Flow reactor

    • M.O.C

SS-316

    • Reaction type

For Homogeneous Reaction-10ml Volume Reactor

For Heterogeneous Reaction- 4ml Volume Reactor

    • Design

For Homogeneous Reaction- ID 1 mm (coiled tube with holder)

For Heterogeneous Reaction- Vol = 4 ml

    • Design Pressure

For Homogeneous Reaction-100 bar

For Heterogeneous Reaction-100 bar

    • Temperature Range

For Homogeneous Reaction- RT to 500 oC

For Heterogeneous Reaction- RT to 500 oC

    • Nozzles & Fittings

For Homogeneous Reaction- OD 1.6 mm

For Heterogeneous Reaction- id = 7 mm, length 100 mm

    • Furnace

Inner material:

The inner of the furnace shall be made from ceramic sheath and the same shall be of 25mm dia.     X 250mm length split in two halves (single zone).

      • Inner Size:

50 mm dia.   X 260 mm Ht.

      • Furnace Outer Size:

200 mm square. X 300 mm Ht.

      • Construction:

The outer of the furnace shall be construction with Stainless steel sheet of 10 SWG (3.0 mm) with buffed finish (2B finish) The furnace shall be split type with SS hinge one side and heavy-duty clamp on other side.

The furnace shall be accommodated in a shell made from mild steel sheet duly powder coated. The same shall be of 250 mm X 450 mm D x 350 mm ht. and shall also house the two-zone control panel on the rear.

      • Heating elements:

The furnace shall have embedded   heating element which shall be high density cartridge heaters of 6mm dia. X 200 mm length which shall be placed on the slots created on a SS 304 machined pipe split into two halves. The same shall be capable of operating at any temperature till 500oC with a control accuracy +/-1*C. The rating of each half shall be 600 watts and shall be 1200W for the whole zone. Total rating shall be 1200W, 230V.

      • Insulation:

The furnace shall be provided with 2ʺ insulation all around comprising of various layer of ceramic wool.

      • Operation Temperature:

500oC

Optional 

Additional PTFE tubing reactor for acid and base reaction (10 ml) 

Photo-chemical reactor (Lamp 250W medium pressure 365 nm lamp, 8W 254 nm lamp, Quartz

Jacket with lamp holder, High purity PFA tubing reactor (10 ml, 50 mL), water circulator).

Optional Accessories

103ml Catalyst Cartridge

103ml Catalyst Cartridge

52ml Catalyst Cartridge

52ml Catalyst Cartridge

7ml Catalyst Cartridge

7ml Catalyst Cartridge

5ml Catalyst Cartridge

5ml Catalyst Cartridge

3ml Catalyst Cartridge

3ml Catalyst Cartridge

1ml Catalyst Cartridge

1ml Catalyst Cartridge

103ml Cartridge Block

103ml Cartridge Block

52ml Cartridge Block

52ml Cartridge Block

7ml, 5ml, 3ml, 1ml Cartridge Block

7ml, 5ml, 3ml, 1ml Cartridge Block

SS-316 10ml 1/8 Tubing Tubular Reactor

SS-316 10ml 1/8 Tubing Tubular Reactor

 PTFE 5ml 1/16 Tubing Tubular Reactor

 PTFE 5ml 1/16 Tubing Tubular Reactor

PTFE10ml 1/16 Tubing Tubular Reactor

PTFE10ml 1/16 Tubing Tubular Reactor

SS-316 10ml 1/16 Tubing Tubular Reactor

SS-316 10ml 1/16 Tubing Tubular Reactor

0.1 Micron SS-316 Filter

0.1 Micron SS-316 Filter

0.2 Micron SS-316 Filter

0.2 Micron SS-316 Filter

Non-Regulating Flow Valves

Non-Regulating Flow Valves

Back Pressure Regulator

Back Pressure Regulator

Ferrule ETFE(TEFZEL)1/16ʺ O.D (SCS-F-E-1/16)

Ferrule ETFE(TEFZEL)1/16ʺ O.D (SCS-F-E-1/16)

Ferrule ETFE (TEFZEL) 1/8ʺ O.D (SCS-F-E-1/8)

Ferrule ETFE (TEFZEL) 1/8ʺ O.D (SCS-F-E-1/8)

Ferrule SS-316 1/16ʺ O.D (SCS-F-SS-1/16)

Ferrule SS-316 1/16ʺ O.D (SCS-F-SS-1/16)

Nut SS-316 1/8ʺ O.D (SCS-N-SS-1/8)

Nut SS-316 1/8ʺ O.D (SCS-N-SS-1/8)

Nut PEEK 1/16ʺ O.D (SCS-N-PK-1/16)

Nut PEEK 1/16ʺ O.D (SCS-N-PK-1/16)

Nut ETFE (TEFZEL) 1/16ʺ O.D (SCS-N-E-1/16)

Nut ETFE (TEFZEL) 1/16ʺ O.D (SCS-N-E-1/16)

Nut 1/8 ETFE (TEFZEL) (SCS-N-E-1/8)

Nut 1/8 ETFE (TEFZEL) (SCS-N-E-1/8)

PTFE Tubing 1/16ʺ O.D (SCS-T-P-1/16)

PTFE Tubing 1/16ʺ O.D (SCS-T-P-1/16)

PTFE Tubing 1/8ʺ O.D (SCS-T-P-1/8)

PTFE Tubing 1/8ʺ O.D (SCS-T-P-1/8)

PTFE Tubing 1/4ʺ O.D (SCS-T-P-1/4)

PTFE Tubing 1/4ʺ O.D (SCS-T-P-1/4)

High Purity PFA Tubing 1/16ʺ O.D (SCS-T-HP-1/16)

High Purity PFA Tubing 1/16ʺ O.D (SCS-T-HP-1/16)

High Purity PFA Tubing 1/8ʺ O.D (SCS-T-HP-1/8)

High Purity PFA Tubing 1/8ʺ O.D (SCS-T-HP-1/8)

SS-316 Tubing 1/16ʺ O.D (SCS-T-SS-1/16)

SS-316 Tubing 1/16ʺ O.D (SCS-T-SS-1/16)

SS-316 Tubing 1/8ʺ O.D (SCS-T-SS-1/8)

SS-316 Tubing 1/8ʺ O.D (SCS-T-SS-1/8)

Y-Junction Nylon (SCS-YJ-N)

Y-Junction Nylon (SCS-YJ-N)

Y-Junction SS-316 (SCS-YJ-SS)

Y-Junction SS-316 (SCS-YJ-SS)

Stainless Steel – 316 Tube Cutter (SCS-SS-TC)

Stainless Steel – 316 Tube Cutter (SCS-SS-TC)

T-Junction Nylon Flat-Bottom (SCS-TJ-N-F)

T-Junction Nylon Flat-Bottom (SCS-TJ-N-F)

T-Junction ETFE (TEFZEL)Flat-Bottom

T-Junction ETFE (TEFZEL)Flat-Bottom

T-Junction PEEK Flat-Bottom (SCS-TJ-PK-F)

T-Junction PEEK Flat-Bottom (SCS-TJ-PK-F)

T-Junction SS-316 Flat-Bottom (SCS-TJ-SS-F)

T-Junction SS-316 Flat-Bottom (SCS-TJ-SS-F)

T-Junction SS-316 Cone Shaped (SCS-TJ-SS-C)

T-Junction SS-316 Cone Shaped (SCS-TJ-SS-C)

Union-Junction Nylon Flat-Bottom (SCS-UJ-N-F)

Union-Junction Nylon Flat-Bottom (SCS-UJ-N-F)

Union-Junction PEEK Flat-Bottom (SCS-UJ-PK-F)

Union-Junction PEEK Flat-Bottom (SCS-UJ-PK-F)

Union-Junction SS-316 Flat-Bottom (SCS-UJ-SS-F)

Union-Junction SS-316 Flat-Bottom (SCS-UJ-SS-F)

Union-Junction SS-316 Cone Shaped (SCS-UJ-SS-C)

Union-Junction SS-316 Cone Shaped (SCS-UJ-SS-C)

X- Junction Nylon (SCS-XJ-N)

X- Junction Nylon (SCS-XJ-N)

X- Junction ETFE (TEFZEL) (SCS-XJ-E)

X- Junction ETFE (TEFZEL) (SCS-XJ-E)

X- Junction PEEK (SCS-XJ-PK )

X- Junction PEEK (SCS-XJ-PK )

X-Junction SS-316 (SCS-XJ-SS)

X-Junction SS-316 (SCS-XJ-SS)