SmartChemSynths all in one photo-chemical flow reactor (SCS-PC)

Liquid-Liquid Separator (SCS-LL)

Either working in batch or flow, extractions dealing with liquid-liquid are hectic. This product module in the flow chemistry is equivalent of a separatory funnel. Continuous Liquid-Liquid separation works on the principle of polarity difference. By using advanced membrane technology rather than gravity, this liquid-liquid flow separator can separate two-phase mixtures i.e. into the aqueous layer and organic layer. This system/device can separate liquids with the same density and emulsions with continuous operation. The separator has excellent performance when operated with two liquids with very low interfacial tension.

Our liquid-liquid flow separator delivers:

  • reduced emulsions compared to batch separation funnels,
  • fast partitioning, phase separation and
  • is easy to use.

Internal Layers of Liquid-Liquid Separator

 

Liquid-Liquid Learning Separator 30ml (SCS-LLL-30)

SmartChemSynths Liquid- Liquid Learning Separator Nylon 30ml (SCS-LLL-30N)

SmartChemSynths Liquid-Liquid Learning Separator SS-316 30ml (SCS-LLL-30SS)

 

Liquid-Liquid learning Separator (SCS-LLL-30) Specifications:

  • Pressure: Upto 2 bar
  • Flow rate: up to 30 ml/min
  • Wetted parts: PTFE
  • Dead volume: 700 µL
  • Maximum operating pressure: 1 bar
  • Temperature Range: 25 to 120 oC
  • Membrane: 0.25-0.45-micron PTFE
  • Inlet/Outlet ports: 1/16, 1/8, 1/4ʺ-28 UNF

 

Liquid-Liquid Pilot Separator 200ml (SCS-LLP-200)

SmartChemSynths Liquid- Liquid Pilot Separator SS-316 200ml (SCS-LLP-200SS)

SmartChemSynths Liquid- Liquid Pilot Separator Nylon 200ml (SCS-LLP-200N)

SCS Liquid-Liquid Pilot Separator (SCS-LLP-30) Specifications:

  • Pressure: Upto 2 bar
  • Flow rate: up to 200 ml/min
  • Wetted parts: PTFE
  • Dead volume: 20 mL
  • Maximum operating pressure: 1 bar
  • Temperature Range: 25 to 120 oC
  • Membrane: 0.25-0.45-micron PTFE
  • Inlet/Outlet ports: 1/8, 1/4ʺ-28 UNF


FUNCTION OF LIQUID-LIQUID SEPARATOR:

When a mixture of two liquids enters the separator composed of aqueous liquid and organic liquid, one phase will have an affinity for the membrane and fill the pores this is referred to as the “wetting” phase), and the other phase will be repelled and will not fill the pores this is referred to as the “non-wetting” phase. Once the membrane pores are filled with the wetting phase, a pressure differential is applied between the two sides of the membrane. The separator is designed to maintain a constant pressure differential across the designated flow rates even when conditions are fluctuating. When a hydrophobic membrane is in place, the organic phase passes through the membrane while the aqueous, which is the non-wetting phase, is retained.

Concept:

The concept of liquid-liquid separator is that it exploits differences in wettability and surface forces to accomplish the separation as a result, the device can separate liquids with the same density and emulsions with continuous operation.

ADVANTAGES

  • The separation can be done faster with this liquid separator compared to batch process, and, thus this increases output of product.
  • Continuous separation can be achieved which speeds up the overall separation.
  • Emulsions and rag layers normally take long periods of time to separate leading to inefficiencies.
  • Liquid-liquid separator allows for easy separation of emulsions by removing the matrix fluid and forcing the emulsion to coalesce.
  • Since separation is density independent, even the most challenging emulsions can be separated with ease.

Sunflower Equivalent Solar Panel Micro-Flow Reactor

Sunflower Equivalent Solar Panel Micro-Flow Reactor

The breakthrough Sun-flower equivalent solar panel micro-flow reactor by Smartchemsynths Machine (OPC) Pvt. Ltd. has wrapped up together the advantages of continuous flow processing with the added benefits of ultraviolet light to enable photochemical reactions.

By eliminating the problems encountered in traditional batch photochemistry, this reactor allows the full potential of photochemistry to be exploited. It offers safe, efficient, and scalable photochemistry under continuous flow operation.

The ultimate light source has been used which is the Sun. The lights fall on the solar panel which placed at a fixed angle to absorb maximum intensity of light. The solar reactor panel is placed in an acrylic box. This solar reactor panel is in series with pump control panel.

Features:

  • Chemically inert tube
  • Easy scale-up
  • Efficient, uniform irradiation
  • Safer in operation

Specifications:

M.O.C

Solar reactor: PFA

Setup box: Acrylic

Pumps: Nylon (Customizable)

Reactor vol.

10ml/min – 1l/min, (customization available as per client requirement)

Flow rate

1µl/min – 20µl/min, (customization available as per client requirement)

Temperature

at RT

Pressure

upto 10bar

Solar panel Stand

Each hole at a displacement angle of 100

Recommended Android App. For measuring light intensity

LUX Light Meter.

Photo– Chemical Flow Reactor

UV Light and Medium Pressure Lamp Output Spectrum

Specifications of Photo-Chemical Flow Reactor:

  • Reactor volume: 1ml -2000 ml
    • Inerr wetted materials: PFA for photo-chemical and PTFE for electrochemical
    • Reactor body- As per requirements (Bakelite, SS-316, PEEK, PTFE, Hasetealloy)
    • pressure: upto 20 bar
    • Optional (batch reactor with 500 ml volume)
  • Syringe pump with variable flow rate:
    • Nano liter to several milliliter/min.
    • Control unit for backward, forward, slow, fast etc.
    • Pump pressure up to 20 bar
  • Plated MS heater with temperature range (240W): RT – 150˚ C.
  • Control panel- Nylon, SS-316, MS
  • Power supply for electrochemistry with fine tuning:
    • Variable current (0-2A), variable voltage (0-29 V).
    • Fix high current and low volt (5A and 12V)
    • Fix low current and high voltage (2A and 110V)
  • Electrodes: Graphite
    • optional: Zinc, Carbon, Copper, Aluminium, Platinum, Stainless Steel mess, Iron, Nickel, Titanium etc)
  • Photochemical reactor (30W LED): Red, Blue, Green, Yellow, Cyan, White light etc.
  • Ultra Violet (UV) Light-254nm (4-40 W)
  • Medium pressure lamp (125-1000 W) 365 nm max.
  • Photo Chemical Reactor:30W LED
  • Quartz Condenser: OD 50mm* Height 300 mm
  • PFA Tubular Reactor 1/16″ O.D
  • Volume: 10ml-100ml
  • Thermal Sensor to measure Temperature 
 

PHOTOCHEMISTRY

The use of this reactor for photochemical applications can overcome most of the issues associated with batch photochemistry. Provides opportunities to ensure a uniform irradiation of the entire reaction mixture. Photochemical reactions are driven by the number of photons that are able to activate molecules causing the desired reaction. Photochemical multiphasic reactions completely exploit the photon- and mass-transfer enhancement properties offered by flow chemistry. Advantages of photochemistry enhanced energy efficiencies and reductions of solvent volumes and consequently waste. The typical setup for photochemical processes comprises transparent body made of acrylic, efficiently coiled with a light source compromising of different colours (wavelength) of light.

Optional Accessories

High Pressure Gas Tight Syringe 25 ml (upto 8 Bar Pressure)

High Pressure Gas Tight Syringe 25 ml (upto 8 Bar Pressure)

High Pressure SS-316 50ml Syringe (upto 50 Bar Pressure)

High Pressure SS-316 50ml Syringe (upto 50 Bar Pressure)

High Pressure SS-316 25ml syringe (upto 50 bar Pressure)

High Pressure SS-316 25ml syringe (upto 50 bar Pressure)

High Pressure SS-316 20ml syringe (upto 50 bar Pressure)

High Pressure SS-316 20ml syringe (upto 50 bar Pressure)

 High Pressure SS-316 6ml Syringe ( upto 100 Bar Pressure)

 High Pressure SS-316 6ml Syringe ( upto 100 Bar Pressure)

Recirculating Pump

Recirculating Pump

UV Light-8W

UV Light-8W

 Photo Chemical Reactor

 Photo Chemical Reactor

Water Recirculating Chamber

Water Recirculating Chamber

Medium pressure lamp 125 W

Medium pressure lamp 125 W

Quartz Jacketed Reactor

Quartz Jacketed Reactor

Ferrule ETFE(TEFZEL)1/16ʺ O.D (SCS-F-E-1/16)

Ferrule ETFE(TEFZEL)1/16ʺ O.D (SCS-F-E-1/16)

Ferrule ETFE (TEFZEL) 1/8ʺ O.D (SCS-F-E-1/8)

Ferrule ETFE (TEFZEL) 1/8ʺ O.D (SCS-F-E-1/8)

Ferrule SS-316 1/16ʺ O.D (SCS-F-SS-1/16)

Ferrule SS-316 1/16ʺ O.D (SCS-F-SS-1/16)

Ferrule SS-316 1/18ʺ O.D (SCS-F-SS-1/8)

Ferrule SS-316 1/18ʺ O.D (SCS-F-SS-1/8)

Nut SS-316 1/16ʺ O.D (SCS-N-SS-1/16)

Nut SS-316 1/16ʺ O.D (SCS-N-SS-1/16)

Nut SS-316 1/8ʺ O.D (SCS-N-SS-1/8)

Nut SS-316 1/8ʺ O.D (SCS-N-SS-1/8)

Nut PEEK 1/16ʺ O.D (SCS-N-PK-1/16)

Nut PEEK 1/16ʺ O.D (SCS-N-PK-1/16)

Nut ETFE (TEFZEL) 1/16ʺ O.D (SCS-N-E-1/16)

Nut ETFE (TEFZEL) 1/16ʺ O.D (SCS-N-E-1/16)

Nut 1/8 ETFE (TEFZEL) (SCS-N-E-1/8)

Nut 1/8 ETFE (TEFZEL) (SCS-N-E-1/8)

PTFE Tubing 1/16ʺ O.D (SCS-T-P-1/16)

PTFE Tubing 1/16ʺ O.D (SCS-T-P-1/16)

PTFE Tubing 1/8ʺ O.D (SCS-T-P-1/8)

PTFE Tubing 1/8ʺ O.D (SCS-T-P-1/8)

PTFE Tubing 1/4ʺ O.D (SCS-T-P-1/4)

PTFE Tubing 1/4ʺ O.D (SCS-T-P-1/4)

High Purity PFA Tubing 1/16ʺ O.D (SCS-T-HP-1/16)

High Purity PFA Tubing 1/16ʺ O.D (SCS-T-HP-1/16)

High Purity PFA Tubing 1/8ʺ O.D (SCS-T-HP-1/8)

High Purity PFA Tubing 1/8ʺ O.D (SCS-T-HP-1/8)

Y-Junction Nylon (SCS-YJ-N)

Y-Junction Nylon (SCS-YJ-N)

Y-Junction SS-316 (SCS-YJ-SS)

Y-Junction SS-316 (SCS-YJ-SS)

T-Junction SS-316 Flat-Bottom (SCS-TJ-SS-F)

T-Junction SS-316 Flat-Bottom (SCS-TJ-SS-F)

T-Junction SS-316 Cone Shaped (SCS-TJ-SS-C)

T-Junction SS-316 Cone Shaped (SCS-TJ-SS-C)

X- Junction Nylon (SCS-XJ-N)

X- Junction Nylon (SCS-XJ-N)

X- Junction ETFE (TEFZEL) (SCS-XJ-E)

X- Junction ETFE (TEFZEL) (SCS-XJ-E)

Union-Junction Nylon Flat-Bottom (SCS-UJ-N-F)

Union-Junction Nylon Flat-Bottom (SCS-UJ-N-F)

Union-Junction PEEK Flat-Bottom (SCS-UJ-PK-F)

Union-Junction PEEK Flat-Bottom (SCS-UJ-PK-F)

X-Junction SS-316 (SCS-XJ-SS)

X-Junction SS-316 (SCS-XJ-SS)