Either working in batch or flow, extractions dealing with liquid-liquid are hectic. This product module in the flow chemistry is equivalent of a separatory funnel. Continuous Liquid-Liquid separation works on the principle of polarity difference. By using advanced membrane technology rather than gravity, this liquid-liquid flow separator can separate two-phase mixtures i.e. into the aqueous layer and organic layer. This system/device can separate liquids with the same density and emulsions with continuous operation. The separator has excellent performance when operated with two liquids with very low interfacial tension.
Our liquid-liquid flow separator delivers:
Internal Layers of Liquid-Liquid Separator
Liquid-Liquid Learning Separator 30ml (SCS-LLL-30)
SmartChemSynths Liquid- Liquid Learning Separator Nylon 30ml (SCS-LLL-30N)
SmartChemSynths Liquid-Liquid Learning Separator SS-316 30ml (SCS-LLL-30SS)
Liquid-Liquid learning Separator (SCS-LLL-30) Specifications:
Liquid-Liquid Pilot Separator 200ml (SCS-LLP-200)
SmartChemSynths Liquid- Liquid Pilot Separator SS-316 200ml (SCS-LLP-200SS)
SmartChemSynths Liquid- Liquid Pilot Separator Nylon 200ml (SCS-LLP-200N)
SCS Liquid-Liquid Pilot Separator (SCS-LLP-30) Specifications:
FUNCTION OF LIQUID-LIQUID SEPARATOR:
When a mixture of two liquids enters the separator composed of aqueous liquid and organic liquid, one phase will have an affinity for the membrane and fill the pores this is referred to as the “wetting” phase), and the other phase will be repelled and will not fill the pores this is referred to as the “non-wetting” phase. Once the membrane pores are filled with the wetting phase, a pressure differential is applied between the two sides of the membrane. The separator is designed to maintain a constant pressure differential across the designated flow rates even when conditions are fluctuating. When a hydrophobic membrane is in place, the organic phase passes through the membrane while the aqueous, which is the non-wetting phase, is retained.
Concept:
The concept of liquid-liquid separator is that it exploits differences in wettability and surface forces to accomplish the separation as a result, the device can separate liquids with the same density and emulsions with continuous operation.
ADVANTAGES
Sunflower Equivalent Solar Panel Micro-Flow Reactor
The breakthrough Sun-flower equivalent solar panel micro-flow reactor by Smartchemsynths Machine (OPC) Pvt. Ltd. has wrapped up together the advantages of continuous flow processing with the added benefits of ultraviolet light to enable photochemical reactions.
By eliminating the problems encountered in traditional batch photochemistry, this reactor allows the full potential of photochemistry to be exploited. It offers safe, efficient, and scalable photochemistry under continuous flow operation.
The ultimate light source has been used which is the Sun. The lights fall on the solar panel which placed at a fixed angle to absorb maximum intensity of light. The solar reactor panel is placed in an acrylic box. This solar reactor panel is in series with pump control panel.
Features:
Specifications:
M.O.C | Solar reactor: PFA Setup box: Acrylic Pumps: Nylon (Customizable) |
Reactor vol. | 10ml/min – 1l/min, (customization available as per client requirement) |
Flow rate | 1µl/min – 20µl/min, (customization available as per client requirement) |
Temperature | at RT |
Pressure | upto 10bar |
Solar panel Stand | Each hole at a displacement angle of 100 |
Recommended Android App. For measuring light intensity | LUX Light Meter. |
SmartChemsynth -Learning Multipurpose Batch/Flow Reactor (SCS-L)
Photochemical light source
Electro Flow Heating Reactor
Our SCS-L Flow/Batch Reactor is an exemplary multi-purpose reactor and specially designed for learning and education purpose. Allows user to cover a wide range of chemical applications. This reactor is user friendly, well designed for the beginners, who are entering into the flow/batch chemistry field. The SCS-L reactor enable its user to perform homogeneous, heterogeneous, high temperature reactions, electrochemical and photochemical reactions as well.
Specifications of Learning Multipurpose Batch/Flow Reactor :
Some more details of the Smartchemsynth Learning Flow Reactor (SCS-L)
Photochemistry
The use of this reactor for photochemical applications can overcome most of the issues associated with batch photochemistry. Provides opportunities to ensure a uniform irradiation of the entire reaction mixture. Photochemical reactions are driven by the number of photons that are able to activate molecules causing the desired reaction. Photochemical multiphasic reactions completely exploit the photon- and mass-transfer enhancement properties offered by flow chemistry. Advantages of photochemistry enhanced energy efficiencies and reductions of solvent volumes and consequently waste. The typical setup for photochemical processes comprises transparent body made of acrylic, efficiently coiled with a light source compromising of different colours (wavelength) of light.
Electrochemistry
In continuous flow process, the transfer of electrons drives reactions and transformations, meaning that electrochemistry is a surface phenomenon whereby reactions are optimised when there is a high surface area to volume ratio. The reduced distance between the electrodes allows better control of the number of electrons transferred to the reaction media, enabling better control and selectivity. It is possible to generate reactive species without the need for hazardous oxidizing and reducing agents.
It is well known that the nature of the electrode material and the over-potential accessible with certain electrodes influence the electrochemical processes. Fine-tuning of electrodes can be very important in order to optimize reactions. Therefore, manipulating electrochemistry in flow gives possible degree of flexibility since the application has control on the flow parameters, the nature of the electrochemical measurement, on the dimensions and nature of the electrode. Benefits of electrochemistry are rapid oxidations and reductions-oxidative synthesis of drug metabolites and oxidative synthesis of drug metabolites.
High Temperature Reactions
There are many chemical reactions in chemistry which need high temperature to reach the desired conversions or yield, till now with traditional batch equipment it is tough, whereas with flow chemistry we can overcome this problem in a very significant way. On increasing the temperature, the rate of reaction increases for many reactions, taking place at around room temperature, and the rate of reaction doubles for every 10 0C rise in temperature.
Homogeneous and Heterogeneous Reactions
The homogeneous & heterogeneous in continuous process offers preferable process control, higher efficiency, and comparable or superior reaction profiles and yields compared to batch conditions.
Applications of Learning Multipurpose Batch/Flow Reactor
Optional Accessories
High Pressure Gas Tight Syringe 25 ml (upto 8 Bar Pressure)
High Pressure Gas Tight Syringe 25 ml (upto 8 Bar Pressure)
High Pressure SS-316 50ml Syringe (upto 50 Bar Pressure)
High Pressure SS-316 50ml Syringe (upto 50 Bar Pressure)
High Pressure SS-316 25ml syringe (upto 50 bar Pressure)
High Pressure SS-316 25ml syringe (upto 50 bar Pressure)
High Pressure SS-316 20ml syringe (upto 50 bar Pressure)
High Pressure SS-316 20ml syringe (upto 50 bar Pressure)
High Pressure SS-316 6ml Syringe ( upto 100 Bar Pressure)
High Pressure SS-316 6ml Syringe ( upto 100 Bar Pressure)
High Purity PFA Tubing 1/16ʺ O.D (SCS-T-HP-1/16)
High Purity PFA Tubing 1/16ʺ O.D (SCS-T-HP-1/16)
Union-Junction SS-316 Flat-Bottom (SCS-UJ-SS-F)
Union-Junction SS-316 Flat-Bottom (SCS-UJ-SS-F)
Union-Junction SS-316 Cone Shaped (SCS-UJ-SS-C)
Union-Junction SS-316 Cone Shaped (SCS-UJ-SS-C)
