Smartchemsynth Gas Separation (SCS-GS) and Analysis Equipment

Liquid-Liquid Separator (SCS-LL)

Either working in batch or flow, extractions dealing with liquid-liquid are hectic. This product module in the flow chemistry is equivalent of a separatory funnel. Continuous Liquid-Liquid separation works on the principle of polarity difference. By using advanced membrane technology rather than gravity, this liquid-liquid flow separator can separate two-phase mixtures i.e. into the aqueous layer and organic layer. This system/device can separate liquids with the same density and emulsions with continuous operation. The separator has excellent performance when operated with two liquids with very low interfacial tension.

Our liquid-liquid flow separator delivers:

  • reduced emulsions compared to batch separation funnels,
  • fast partitioning, phase separation and
  • is easy to use.

Internal Layers of Liquid-Liquid Separator

 

Liquid-Liquid Learning Separator 30ml (SCS-LLL-30)

SmartChemSynths Liquid- Liquid Learning Separator Nylon 30ml (SCS-LLL-30N)

SmartChemSynths Liquid-Liquid Learning Separator SS-316 30ml (SCS-LLL-30SS)

 

Liquid-Liquid learning Separator (SCS-LLL-30) Specifications:

  • Pressure: Upto 2 bar
  • Flow rate: up to 30 ml/min
  • Wetted parts: PTFE
  • Dead volume: 700 µL
  • Maximum operating pressure: 1 bar
  • Temperature Range: 25 to 120 oC
  • Membrane: 0.25-0.45-micron PTFE
  • Inlet/Outlet ports: 1/16, 1/8, 1/4ʺ-28 UNF

 

Liquid-Liquid Pilot Separator 200ml (SCS-LLP-200)

SmartChemSynths Liquid- Liquid Pilot Separator SS-316 200ml (SCS-LLP-200SS)

SmartChemSynths Liquid- Liquid Pilot Separator Nylon 200ml (SCS-LLP-200N)

SCS Liquid-Liquid Pilot Separator (SCS-LLP-30) Specifications:

  • Pressure: Upto 2 bar
  • Flow rate: up to 200 ml/min
  • Wetted parts: PTFE
  • Dead volume: 20 mL
  • Maximum operating pressure: 1 bar
  • Temperature Range: 25 to 120 oC
  • Membrane: 0.25-0.45-micron PTFE
  • Inlet/Outlet ports: 1/8, 1/4ʺ-28 UNF


FUNCTION OF LIQUID-LIQUID SEPARATOR:

When a mixture of two liquids enters the separator composed of aqueous liquid and organic liquid, one phase will have an affinity for the membrane and fill the pores this is referred to as the “wetting” phase), and the other phase will be repelled and will not fill the pores this is referred to as the “non-wetting” phase. Once the membrane pores are filled with the wetting phase, a pressure differential is applied between the two sides of the membrane. The separator is designed to maintain a constant pressure differential across the designated flow rates even when conditions are fluctuating. When a hydrophobic membrane is in place, the organic phase passes through the membrane while the aqueous, which is the non-wetting phase, is retained.

Concept:

The concept of liquid-liquid separator is that it exploits differences in wettability and surface forces to accomplish the separation as a result, the device can separate liquids with the same density and emulsions with continuous operation.

ADVANTAGES

  • The separation can be done faster with this liquid separator compared to batch process, and, thus this increases output of product.
  • Continuous separation can be achieved which speeds up the overall separation.
  • Emulsions and rag layers normally take long periods of time to separate leading to inefficiencies.
  • Liquid-liquid separator allows for easy separation of emulsions by removing the matrix fluid and forcing the emulsion to coalesce.
  • Since separation is density independent, even the most challenging emulsions can be separated with ease.

Sunflower Equivalent Solar Panel Micro-Flow Reactor

Sunflower Equivalent Solar Panel Micro-Flow Reactor

The breakthrough Sun-flower equivalent solar panel micro-flow reactor by Smartchemsynths Machine (OPC) Pvt. Ltd. has wrapped up together the advantages of continuous flow processing with the added benefits of ultraviolet light to enable photochemical reactions.

By eliminating the problems encountered in traditional batch photochemistry, this reactor allows the full potential of photochemistry to be exploited. It offers safe, efficient, and scalable photochemistry under continuous flow operation.

The ultimate light source has been used which is the Sun. The lights fall on the solar panel which placed at a fixed angle to absorb maximum intensity of light. The solar reactor panel is placed in an acrylic box. This solar reactor panel is in series with pump control panel.

Features:

  • Chemically inert tube
  • Easy scale-up
  • Efficient, uniform irradiation
  • Safer in operation

Specifications:

M.O.C

Solar reactor: PFA

Setup box: Acrylic

Pumps: Nylon (Customizable)

Reactor vol.

10ml/min – 1l/min, (customization available as per client requirement)

Flow rate

1µl/min – 20µl/min, (customization available as per client requirement)

Temperature

at RT

Pressure

upto 10bar

Solar panel Stand

Each hole at a displacement angle of 100

Recommended Android App. For measuring light intensity

LUX Light Meter.

Smartchemsynth Gas Separation (SCS-GS) and Analysis Equipment

Smart Flow Reactor

Specifications of Smart Flow Reactor:

Catalyst Cartridge
M.O.C : SS-316
Reaction type: Gas-gas separation
Total Reactor Volume: 4 ml
Design: ID 3 mm (coiled tube with holder)
Design Pressure: 100 bar
Temperature Range: RT to 500 oC
Nozzles & Fittings: OD 1.6 mm

Furnace

Specifications of Furnace

  • Inner material:
      The inner of the furnace shall be made from ceramic sheath and the same shall be of 25mm dia. X 250mm length split in two halves (single zone).
  • Inner Size:
      50 mm dia.   X 260 mm Ht.
  • Furnace Outer Size:
      200 mm square. X 300 mm Ht.
  • Construction:
      • The outer of the furnace shall be construction with Stainless steel sheet of 10 SWG (3.0 mm) with buffed finish (2B finish) The furnace shall be split type with SS hinge one side and heavy duty clamp on other side.

     

    The furnace shall be accommodated in a shell made from mild steel sheet duly powder coated. The same shall be of 250 mm X 450 mm D x 350 mm ht. and shall also house the two zone control panel on the rear.

  • Heating elements:

    The furnace shall have embedded   heating element which shall be high density cartridge heaters of 6mm dia. X 200 mm length which shall be placed on the slots created on a SS 304 machined pipe split into two halves. The same shall be capable of operating at any temperature till 500*C with a control accuracy +/-1*C. The rating of each half shall be 600 watts and shall be 1200W for the whole zone. Total rating shall be 1200W, 230V.

  • Insulation:

    The furnace shall be provided with 2ʺ insulation all around comprising of various layer of ceramic wool.

  • Operation Temperature:
      500*C
  • Mass Flow Controller:
      • Thermal Mass-Flow Controller ALUMINUM Viton-a seals 1/16″Compression fitting LCD Display NA/4-20mA

     

    0-100 Standard ML/Min Standard Metering Pressure (14.7Psia) Standard Temperature (21.1˚ C)

 GC-TCD/FID

Specifications of GC-TCD/FID

Nucon Series 5765 digital Dual column Gas Chromatograph with:

DUAL FLAME IONISATION DETECTOR:- Microprocessor controls with keyboard entry of process parameters and timing functions with user friendly software in ROM, method development facility and electricity failure back up. Automatic Temperature programming facility with four RAMPS for Oven. Intial mid and final timing and auxiliary temperature Control channel besides oven. Injector and Detector with Auto Dignostics facility & AUTO COOLING FACILITY completete with necessary standard accessories.

WITH BELOW CONFIGURATION:-

  1. Dual FID single out put with shielding wire with platinum electrode for stability s and noise less signal
  2. TCD
  3. Dual packed column injector ports
  4. Single channel chromatography interface winchrom with software (window based) to be used with your pc

GAS CHROMATOGRAPH WITH BELOW FEATURE: –

All glass system

FID quartz jet

Proven modular system

Imported Cat ridge heaters for base body heating

Platinum temperature sensors

Microprocessor based digital temperature controller

State of art modular chromatography

Wide range of detectors & Automation capability

Provision for two packed / capillary columns

Provision for mechanizer, cryogenic attachment

Multidimensional chromatography

Full line of valves

Modular system, all individual modules like oven, fid & tcd and

data station and computer, printer

Digital Temperature Monitoring for Injector, Oven, Detector and Auxiliary channel of any  Swagelok Type International Standard Stainless Steel

Connectors

Output on Terminals for Recorder, Integrator and Data Station

Provided

5 ramp operation, 9 method files for programmable data storage

Auto Diagnostics facility & auto cooling facility

Auto repeat Runs 0- 999

Programming rate 0- 29.9 oC in 0.1 oC step

Provision for Auxiliary temperature controls for feature up gradation GC with any detector

Provision for feature up gradation of any modules like cryogenic attachment, head space attachment and others detector and temperature controllers

All data will be stored and retrieved from the computer at any time

 NRV

Specifications of NRV:

 Spring based NRV:

Locking with viton Wetting part PTFE Cracking pressure 2 bar

Valve (Manual Valve)

Specifications of Valve:

Material: PTFE
Working Pressure: 1.6-6.4mpa
Working Temperature: -29 oC — +180 oC
Operation Temperature: -10 oC ~150 oC

Optional Accessories

103ml Catalyst Cartridge

103ml Catalyst Cartridge

52ml Catalyst Cartridge

52ml Catalyst Cartridge

7ml Catalyst Cartridge

7ml Catalyst Cartridge

5ml Catalyst Cartridge

5ml Catalyst Cartridge

3ml Catalyst Cartridge

3ml Catalyst Cartridge

1ml Catalyst Cartridge

1ml Catalyst Cartridge

103ml Cartridge Block

103ml Cartridge Block

52ml Cartridge Block

52ml Cartridge Block

7ml, 5ml, 3ml, 1ml Cartridge Block

7ml, 5ml, 3ml, 1ml Cartridge Block

 PTFE 5ml 1/16 Tubing Tubular Reactor

 PTFE 5ml 1/16 Tubing Tubular Reactor

PTFE10ml 1/16 Tubing Tubular Reactor

PTFE10ml 1/16 Tubing Tubular Reactor

SS-316 5ml 1/16 Tubing Tubular Reactor

SS-316 5ml 1/16 Tubing Tubular Reactor

SS-316 10ml 1/16 Tubing Tubular Reactor

SS-316 10ml 1/16 Tubing Tubular Reactor

SS-316 10ml 1/8 Tubing Tubular Reactor

SS-316 10ml 1/8 Tubing Tubular Reactor

0.2 Micron SS-316 Filter (22mm Dia)

0.2 Micron SS-316 Filter (22mm Dia)

0.1 Micron SS-316 Filter

0.1 Micron SS-316 Filter

0.2 Micron SS-316 Filter

0.2 Micron SS-316 Filter