Smartchemsynth Electrochemical Reactor (SCS-EB)

Liquid-Liquid Separator (SCS-LL)

Either working in batch or flow, extractions dealing with liquid-liquid are hectic. This product module in the flow chemistry is equivalent of a separatory funnel. Continuous Liquid-Liquid separation works on the principle of polarity difference. By using advanced membrane technology rather than gravity, this liquid-liquid flow separator can separate two-phase mixtures i.e. into the aqueous layer and organic layer. This system/device can separate liquids with the same density and emulsions with continuous operation. The separator has excellent performance when operated with two liquids with very low interfacial tension.

Our liquid-liquid flow separator delivers:

  • reduced emulsions compared to batch separation funnels,
  • fast partitioning, phase separation and
  • is easy to use.

Internal Layers of Liquid-Liquid Separator

 

Liquid-Liquid Learning Separator 30ml (SCS-LLL-30)

SmartChemSynths Liquid- Liquid Learning Separator Nylon 30ml (SCS-LLL-30N)

SmartChemSynths Liquid-Liquid Learning Separator SS-316 30ml (SCS-LLL-30SS)

 

Liquid-Liquid learning Separator (SCS-LLL-30) Specifications:

  • Pressure: Upto 2 bar
  • Flow rate: up to 30 ml/min
  • Wetted parts: PTFE
  • Dead volume: 700 µL
  • Maximum operating pressure: 1 bar
  • Temperature Range: 25 to 120 oC
  • Membrane: 0.25-0.45-micron PTFE
  • Inlet/Outlet ports: 1/16, 1/8, 1/4ʺ-28 UNF

 

Liquid-Liquid Pilot Separator 200ml (SCS-LLP-200)

SmartChemSynths Liquid- Liquid Pilot Separator SS-316 200ml (SCS-LLP-200SS)

SmartChemSynths Liquid- Liquid Pilot Separator Nylon 200ml (SCS-LLP-200N)

SCS Liquid-Liquid Pilot Separator (SCS-LLP-30) Specifications:

  • Pressure: Upto 2 bar
  • Flow rate: up to 200 ml/min
  • Wetted parts: PTFE
  • Dead volume: 20 mL
  • Maximum operating pressure: 1 bar
  • Temperature Range: 25 to 120 oC
  • Membrane: 0.25-0.45-micron PTFE
  • Inlet/Outlet ports: 1/8, 1/4ʺ-28 UNF


FUNCTION OF LIQUID-LIQUID SEPARATOR:

When a mixture of two liquids enters the separator composed of aqueous liquid and organic liquid, one phase will have an affinity for the membrane and fill the pores this is referred to as the “wetting” phase), and the other phase will be repelled and will not fill the pores this is referred to as the “non-wetting” phase. Once the membrane pores are filled with the wetting phase, a pressure differential is applied between the two sides of the membrane. The separator is designed to maintain a constant pressure differential across the designated flow rates even when conditions are fluctuating. When a hydrophobic membrane is in place, the organic phase passes through the membrane while the aqueous, which is the non-wetting phase, is retained.

Concept:

The concept of liquid-liquid separator is that it exploits differences in wettability and surface forces to accomplish the separation as a result, the device can separate liquids with the same density and emulsions with continuous operation.

ADVANTAGES

  • The separation can be done faster with this liquid separator compared to batch process, and, thus this increases output of product.
  • Continuous separation can be achieved which speeds up the overall separation.
  • Emulsions and rag layers normally take long periods of time to separate leading to inefficiencies.
  • Liquid-liquid separator allows for easy separation of emulsions by removing the matrix fluid and forcing the emulsion to coalesce.
  • Since separation is density independent, even the most challenging emulsions can be separated with ease.

Sunflower Equivalent Solar Panel Micro-Flow Reactor

Sunflower Equivalent Solar Panel Micro-Flow Reactor

The breakthrough Sun-flower equivalent solar panel micro-flow reactor by Smartchemsynths Machine (OPC) Pvt. Ltd. has wrapped up together the advantages of continuous flow processing with the added benefits of ultraviolet light to enable photochemical reactions.

By eliminating the problems encountered in traditional batch photochemistry, this reactor allows the full potential of photochemistry to be exploited. It offers safe, efficient, and scalable photochemistry under continuous flow operation.

The ultimate light source has been used which is the Sun. The lights fall on the solar panel which placed at a fixed angle to absorb maximum intensity of light. The solar reactor panel is placed in an acrylic box. This solar reactor panel is in series with pump control panel.

Features:

  • Chemically inert tube
  • Easy scale-up
  • Efficient, uniform irradiation
  • Safer in operation

Specifications:

M.O.C

Solar reactor: PFA

Setup box: Acrylic

Pumps: Nylon (Customizable)

Reactor vol.

10ml/min – 1l/min, (customization available as per client requirement)

Flow rate

1µl/min – 20µl/min, (customization available as per client requirement)

Temperature

at RT

Pressure

upto 10bar

Solar panel Stand

Each hole at a displacement angle of 100

Recommended Android App. For measuring light intensity

LUX Light Meter.

Electrochemical Reactor Control Panel

Batch Electrolysis Reactor

Specifications of Electrochemical Reactor (SCS-EB):

  • Control Panel-Nylon
  • Power Supply for Electrochemistry with fine tuning:
    • Variable Current (0-2A), Variable Voltage (0-28V)
  • Electrodes: Zinc, Carbon, Graphite, Copper, Aluminium etc. (as per requirement)

Electrochemistry:

In continuous flow process, the transfer of electrons drives reactions and transformations, meaning that electrochemistry is a surface phenomenon whereby reactions are optimised when there is a high surface area to volume ratio. The reduced distance between the electrodes allows better control of the number of electrons transferred to the reaction media, enabling better control and selectivity. It is possible to generate reactive species without the need for hazardous oxidizing and reducing agents.

It is well known that the nature of the electrode material and the over-potential accessible with certain electrodes influence the electrochemical processes. Fine-tuning of electrodes can be very important in order to optimize reactions. Therefore, manipulating electrochemistry in flow gives possible degree of flexibility since the application has control on the flow parameters, the nature of the electrochemical measurement, on the dimensions and nature of the electrode. Benefits of electrochemistry are rapid oxidations and reductions-oxidative synthesis of drug metabolites and oxidative synthesis of drug metabolites.

Optional Accessories

Batch Electrode Assembly 

Batch Electrode Assembly 

Copper Electrode

Copper Electrode

Brass Electrode

Brass Electrode

Tin Electrode 

Tin Electrode 

Lead Electrode

Lead Electrode

Graphite Electrode

Graphite Electrode

Aluminium Electrode

Aluminium Electrode

SS-316 Electrode

SS-316 Electrode

Iron Electrode

Iron Electrode

Nickel Electrode

Nickel Electrode

Cu@Ni Electrode

Cu@Ni Electrode

Zinc Electrode

Zinc Electrode

Glass Test Tube

Glass Test Tube

Batch Reactor Holder (PTFE, Nylon)

Batch Reactor Holder (PTFE, Nylon)