Hydrogen Generator – smartchemsynths

Smartchemsynth Continuous Flow Hydrogenation Reactor (SCS-HG)

Liquid-Liquid Separator (SCS-LL)

Either working in batch or flow, extractions dealing with liquid-liquid are hectic. This product module in the flow chemistry is equivalent of a separatory funnel. Continuous Liquid-Liquid separation works on the principle of polarity difference. By using advanced membrane technology rather than gravity, this liquid-liquid flow separator can separate two-phase mixtures i.e. into the aqueous layer and organic layer. This system/device can separate liquids with the same density and emulsions with continuous operation. The separator has excellent performance when operated with two liquids with very low interfacial tension.

Our liquid-liquid flow separator delivers:

reduced emulsions compared to batch separation funnels,
fast partitioning, phase separation and
is easy to use.

Internal Layers of Liquid-Liquid Separator

Liquid-Liquid Learning Separator 30ml (SCS-LLL-30)

SmartChemSynths Liquid- Liquid Learning Separator Nylon 30ml (SCS-LLL-30N)

SmartChemSynths Liquid-Liquid Learning Separator SS-316 30ml (SCS-LLL-30SS)

Liquid-Liquid learning Separator (SCS-LLL-30) Specifications:

Pressure: Upto 2 bar
Flow rate: up to 30 ml/min
Wetted parts: PTFE
Dead volume: 700 µL
Maximum operating pressure: 1 bar
Temperature Range: 25 to 120 ^oC
Membrane: 0.25-0.45-micron PTFE
Inlet/Outlet ports: 1/16, 1/8, 1/4ʺ-28 UNF

Liquid-Liquid Pilot Separator 200ml (SCS-LLP-200)

SmartChemSynths Liquid- Liquid Pilot Separator SS-316 200ml (SCS-LLP-200SS)

SmartChemSynths Liquid- Liquid Pilot Separator Nylon 200ml (SCS-LLP-200N)

SCS Liquid-Liquid Pilot Separator (SCS-LLP-30) Specifications:

Pressure: Upto 2 bar
Flow rate: up to 200 ml/min
Wetted parts: PTFE
Dead volume: 20 mL
Maximum operating pressure: 1 bar
Temperature Range: 25 to 120 ^oC
Membrane: 0.25-0.45-micron PTFE
Inlet/Outlet ports: 1/8, 1/4ʺ-28 UNF

FUNCTION OF LIQUID-LIQUID SEPARATOR:

When a mixture of two liquids enters the separator composed of aqueous liquid and organic liquid, one phase will have an affinity for the membrane and fill the pores this is referred to as the “wetting” phase), and the other phase will be repelled and will not fill the pores this is referred to as the “non-wetting” phase. Once the membrane pores are filled with the wetting phase, a pressure differential is applied between the two sides of the membrane. The separator is designed to maintain a constant pressure differential across the designated flow rates even when conditions are fluctuating. When a hydrophobic membrane is in place, the organic phase passes through the membrane while the aqueous, which is the non-wetting phase, is retained.

Concept:

The concept of liquid-liquid separator is that it exploits differences in wettability and surface forces to accomplish the separation as a result, the device can separate liquids with the same density and emulsions with continuous operation.

ADVANTAGES

The separation can be done faster with this liquid separator compared to batch process, and, thus this increases output of product.
Continuous separation can be achieved which speeds up the overall separation.
Emulsions and rag layers normally take long periods of time to separate leading to inefficiencies.
Liquid-liquid separator allows for easy separation of emulsions by removing the matrix fluid and forcing the emulsion to coalesce.
Since separation is density independent, even the most challenging emulsions can be separated with ease.

Sunflower Equivalent Solar Panel Micro-Flow Reactor

The breakthrough Sun-flower equivalent solar panel micro-flow reactor by Smartchemsynths Machine (OPC) Pvt. Ltd. has wrapped up together the advantages of continuous flow processing with the added benefits of ultraviolet light to enable photochemical reactions.

By eliminating the problems encountered in traditional batch photochemistry, this reactor allows the full potential of photochemistry to be exploited. It offers safe, efficient, and scalable photochemistry under continuous flow operation.

The ultimate light source has been used which is the Sun. The lights fall on the solar panel which placed at a fixed angle to absorb maximum intensity of light. The solar reactor panel is placed in an acrylic box. This solar reactor panel is in series with pump control panel.

Features:

Chemically inert tube
Easy scale-up
Efficient, uniform irradiation
Safer in operation

Specifications:

M.O.C	Solar reactor: PFA Setup box: Acrylic Pumps: Nylon (Customizable)
Reactor vol.	10ml/min – 1l/min, (customization available as per client requirement)
Flow rate	1µl/min – 20µl/min, (customization available as per client requirement)
Temperature	at RT
Pressure	upto 10bar
Solar panel Stand	Each hole at a displacement angle of 10⁰
Recommended Android App. For measuring light intensity	LUX Light Meter.

Multipurpose High Temperature and High pressure sloid – Liquid Reactor

HPLC

MFC

DESCRIPTION:

Hydrogen Generator setup consists of:

Multipurpose High Temperature and High Pressure Solid-Liquid Reactor
HPLC Pump
Mass Flow Controller
Catalyst Cartridges
Non Regulating Valve (NRV) and Back Pressure Regulator (BPR)

Specifications of Multipurpose High Temperature and High Pressure Solid-Liquid Reactor

Smart flow reactor: Multi-purpose Flow reactor
O.C: SS-316
Reaction type:

Design: For Homogeneous Reaction- ID 1 mm (coiled tube with holder)

Design Pressure: For Homogeneous Reaction-100 bar

Temperature Range: For Homogeneous Reaction- RT to 500^oC

Nozzles & Fittings: For Homogeneous Reaction- OD 1.6 mm

Furnace:
- Inner material: The inner of the furnace shall be made from ceramic sheath and the same shall be of 25mm dia. X 250mm length split in two halves (single zone).
- Inner Size: 50 mm dia. X 260 mm Ht.
- Furnace Outer Size: 200 mm square. X 300 mm Ht.
- Non Regulating Valve (NRV): 1-3 bar pressure (fixed)
- Back Pressure Regulator (BPR): 0-upto 70 bar pressure (variable)
- Catalyst Cartridges: 103ml,52ml,7ml

HPLC PUMP

Specifications of HPLC Pump:

Pump: Pump P 4.1S with 50 ml pump head (stainless steel), pressure sensor P 4.1S, 50 ml, stainless steel
flow rate: 50ml/min
Flow rate range: 01-50 ml/min
Flow rate increment: 01
Maximum delivery pressure: 2180 psi
Maximum delivery pressure (bar): 150
Maximum delivery pressure (MPa): 15MPa
Pressure range: 150bar
Pump head material: Stainless steel
Maximum viscosity: 100cp
Liquid temperature range: 4-60 °C (39.2-140 °F)
Gradient: Isocratic
Leak management: No
Wetted materials: GFP (graphite fiber reinforced PTFE), ruby, sapphire, Titanium

Note: Pressure sensor membrane made of stainless steel;lmitted wetting in fluidic path

Best working conditions: 0-40.0 ml/min
Continuous working conditions: 3-25 ml/min
Flow rate accuracy: 2%
Flow rate accuracy conditions: 5-50% flow rate using ethanol/water 10:90
Flow rate precision: 5% RSD
Flow rate precision conditions: Measured at 1 ml/min using ethanol/water 10:90
Pump type: Ultra-compact high-pressure pump
Pulsation compensation: No
Active piston seal wash: No
Piston seal washing: Yes
System protection: Pmin and Pmax adjustable

Imin and Imax adjustable

Pump head inlet(standard): 1/4”-28 UNF (flat bottom)
Pump head outlet(standard): 10-32 UNF (coned)
Interfaces: Display
Control: RS -232; analog, button on device
Analog inputs: 0-10V
Power supply: 100-240V; 50-60 Hz
Dimensions: 121 x 129 x 220 mm
Weight: 3 kgs
Leak sensor: No
Ambient conditions: Temperature range 10-40°C; 50-104°F
Air humidity: below 90% (non condensing)

MASS FLOW CONTROLER:

Specifications of Mass Flow Controller:

Model: GFC 17
Flow rate range: 0-500 ml/min minimum starts from 12.5 ml/min and max 500ml/min
Flow range: 0-100%
Accuracy: %
Calibrations: Performed at standard conditions [14.7 psia (101.4 kPa) and 70 °F (21.1 °C)] unless otherwise requested.
Repeatability: ±0.5% of full scale.
Response time: 300ms time constant; approximately 1 second to within ±2% of set flow rate for 25% to 100% of full-scale flow.
Temperature coefficient: 15% of full scale / °C.
Pressure coefficient: 01% of full scale / psi (0.07 bar).
Optimum gas pressure: 25 psig (1.73 bars).
Gas pressure: 1000 psig (70 bars) maximum
Turn down ratio: 40:1.
Diff. Pressure: 50 psi
Gas and ambient temp: 32 °F to 122 °F (0 °C to 50 °C). 14 °F to 122 °F (-10 °C to 50 °C) – Dry gases only.
Materials In fluid contact: Stainless steel
Attitude sensitivity: No greater than +15-degree rotation from horizontal to vertical; standard calibration is in horizontal position.
Output signals: Linear 0-5V DC. (1000 ohms min. load impedance); 4-20 mA (0-500 ohms loop resistance) Max noise ±20mV.
Command signals: Analog 0-5V DC or 4-20 mA for remote set point mode; NPN compatible purge /valve off.
Connections: 1/4″ compression fittings. Optional: 6mm, 3/8″ and 1/8″ compression fittings or 1/4″ VCR®
Leak integrity: 1 x 10-9 smL/sec of helium maximum to the outside environment.
Transducer Input power: Universal +12 Vdc to 26 Vdc, 650 mA maximum.
Circuit protection: Circuit boards have built-in polarity reversal protection. Resettable fuses provide power input protection.
Display: 3-1/2-digit LCD, 0.5″ high characters.