Diazo-M-Pen and Diazo Quencher

Liquid-Liquid Separator (SCS-LL)

Either working in batch or flow, extractions dealing with liquid-liquid are hectic. This product module in the flow chemistry is equivalent of a separatory funnel. Continuous Liquid-Liquid separation works on the principle of polarity difference. By using advanced membrane technology rather than gravity, this liquid-liquid flow separator can separate two-phase mixtures i.e. into the aqueous layer and organic layer. This system/device can separate liquids with the same density and emulsions with continuous operation. The separator has excellent performance when operated with two liquids with very low interfacial tension.

Our liquid-liquid flow separator delivers:

  • reduced emulsions compared to batch separation funnels,
  • fast partitioning, phase separation and
  • is easy to use.

Internal Layers of Liquid-Liquid Separator

 

Liquid-Liquid Learning Separator 30ml (SCS-LLL-30)

SmartChemSynths Liquid- Liquid Learning Separator Nylon 30ml (SCS-LLL-30N)

SmartChemSynths Liquid-Liquid Learning Separator SS-316 30ml (SCS-LLL-30SS)

 

Liquid-Liquid learning Separator (SCS-LLL-30) Specifications:

  • Pressure: Upto 2 bar
  • Flow rate: up to 30 ml/min
  • Wetted parts: PTFE
  • Dead volume: 700 µL
  • Maximum operating pressure: 1 bar
  • Temperature Range: 25 to 120 oC
  • Membrane: 0.25-0.45-micron PTFE
  • Inlet/Outlet ports: 1/16, 1/8, 1/4ʺ-28 UNF

 

Liquid-Liquid Pilot Separator 200ml (SCS-LLP-200)

SmartChemSynths Liquid- Liquid Pilot Separator SS-316 200ml (SCS-LLP-200SS)

SmartChemSynths Liquid- Liquid Pilot Separator Nylon 200ml (SCS-LLP-200N)

SCS Liquid-Liquid Pilot Separator (SCS-LLP-30) Specifications:

  • Pressure: Upto 2 bar
  • Flow rate: up to 200 ml/min
  • Wetted parts: PTFE
  • Dead volume: 20 mL
  • Maximum operating pressure: 1 bar
  • Temperature Range: 25 to 120 oC
  • Membrane: 0.25-0.45-micron PTFE
  • Inlet/Outlet ports: 1/8, 1/4ʺ-28 UNF


FUNCTION OF LIQUID-LIQUID SEPARATOR:

When a mixture of two liquids enters the separator composed of aqueous liquid and organic liquid, one phase will have an affinity for the membrane and fill the pores this is referred to as the “wetting” phase), and the other phase will be repelled and will not fill the pores this is referred to as the “non-wetting” phase. Once the membrane pores are filled with the wetting phase, a pressure differential is applied between the two sides of the membrane. The separator is designed to maintain a constant pressure differential across the designated flow rates even when conditions are fluctuating. When a hydrophobic membrane is in place, the organic phase passes through the membrane while the aqueous, which is the non-wetting phase, is retained.

Concept:

The concept of liquid-liquid separator is that it exploits differences in wettability and surface forces to accomplish the separation as a result, the device can separate liquids with the same density and emulsions with continuous operation.

ADVANTAGES

  • The separation can be done faster with this liquid separator compared to batch process, and, thus this increases output of product.
  • Continuous separation can be achieved which speeds up the overall separation.
  • Emulsions and rag layers normally take long periods of time to separate leading to inefficiencies.
  • Liquid-liquid separator allows for easy separation of emulsions by removing the matrix fluid and forcing the emulsion to coalesce.
  • Since separation is density independent, even the most challenging emulsions can be separated with ease.

Sunflower Equivalent Solar Panel Micro-Flow Reactor

Sunflower Equivalent Solar Panel Micro-Flow Reactor

The breakthrough Sun-flower equivalent solar panel micro-flow reactor by Smartchemsynths Machine (OPC) Pvt. Ltd. has wrapped up together the advantages of continuous flow processing with the added benefits of ultraviolet light to enable photochemical reactions.

By eliminating the problems encountered in traditional batch photochemistry, this reactor allows the full potential of photochemistry to be exploited. It offers safe, efficient, and scalable photochemistry under continuous flow operation.

The ultimate light source has been used which is the Sun. The lights fall on the solar panel which placed at a fixed angle to absorb maximum intensity of light. The solar reactor panel is placed in an acrylic box. This solar reactor panel is in series with pump control panel.

Features:

  • Chemically inert tube
  • Easy scale-up
  • Efficient, uniform irradiation
  • Safer in operation

Specifications:

M.O.C

Solar reactor: PFA

Setup box: Acrylic

Pumps: Nylon (Customizable)

Reactor vol.

10ml/min – 1l/min, (customization available as per client requirement)

Flow rate

1µl/min – 20µl/min, (customization available as per client requirement)

Temperature

at RT

Pressure

upto 10bar

Solar panel Stand

Each hole at a displacement angle of 100

Recommended Android App. For measuring light intensity

LUX Light Meter.

daizompen1

Batch Electrolysis Reactor

Diazomethane has a vast range of applications such as in the multi-step synthesis of drugs and natural products, includes bactericides and pesticides, and functional chemicals, solvent for polymerization reactions, formation of API intermediates such as sitagliptin, etc.

Despite its wide synthetic versatility, diazomethane is a highly hazardous reagent because of its carcinogenic, allergen, toxic and explosive nature. Diazomethane can be synthesized now in an ultra-fast continuous flow reactor system on a laboratory scale by our DIAZO-PEN, with little or no danger of explosion.

Specifications of Diazo M-Pen

M.O.C: Syringe: PTFE (customization available in Glass, SS and Hastelloy)

Setup Box: Nylon (customization available in MS, PTFE, SS and Hastelloy)

Pump Flowrate: 10µl/min – 50ml/min

(customization of flowrate available from nanolitre/min – litre/min)

Pressure: upto 6bar (customizable upto 20bar)

Temperature: Room Temperature

Diazo-Quencher

Specially designed cotton-fibre mask is for safety of the chemist to prevent from much exposure to Diazo-methane. If a person gets exposed to 10 ppm in a day to this lethal Diazo-methane, then the person would be in danger. This mask works on by changing colour. Initial colour is metallic light blue, on exposure to Diazomethane it keeps changing colour from blue to green and finally to black. The mask colour switches to green   one is expected to avoid engagement with Diazomethane. Black colour gives indication that the toxicity limit has reached its farthest point, it is an alarm sign for a person being exposed to diazomethane. We recommend our users to buy Diazo-mask, if they come in contact with Diazomethane a lot.